Hplc columns
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HPLC COLUMNS
Allure ®
Columns: 5μm particles; 60Å pore size Small pore size in a high-purity, Type B silica provides a large surface area. High carbon
loads, highly retentive. An excellent choice for light scattering (ELSD) and MS detectors,
in which more organic solvent in the mobile phase gives better sensitivity.
Allure® C18 Columns (USP L1) Excellent Columns for LC/MS and ELSD Physical Characteristics:
Chromatographic Properties:
Most retentive of our alkyl stationary phases due to large surface area of the base silica andhigh-density bondings. Provides excellent peak shapes for a wide range of compounds.
Application . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .Page #
Antibiotics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .526
Herbicides . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .504
Pesticides . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .506
Allure® Basix Columns (USP L10) Excellent Columns for LC/MS and ELSD Physical Characteristics:
Application . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .Page #
Chromatographic Properties:
Acetaminophen, Narcotic Analgesics . . . . . . . . . . . . .519
Highly retentive propyl cyano phase. Excellent choice for basic compounds and for analytes
Albuterol . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .528
containing amine group functionality.
Antiarrhythmics . . . . . . . . . . . . . . . . . . . . . . . . . .521, 522
Antibiotics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .526
Antidepressants . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .527
Herbicides . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .503
Ibuprofen & Pseudoephedrine . . . . . . . . . . . . . . . . . .533
Sedatives . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .532
Steroids . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .530
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HPLC COLUMNS
Allure® PFP Propyl Columns (USP L43) Excellent Columns for LC/MS and ELSD Physical Characteristics:
Chromatographic Properties:
A pentafluorophenyl phase with a propyl spacer. Highly retentive for basic analytes. An excellent phase for separating nucleosides, nucleotides, purines, pyrimidines, halogenatedcompounds, β-blockers, and tricyclic antidepressants.
Application . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .Page #
Antibiotics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .524
Benzodiazepines . . . . . . . . . . . . . . . . . . . . . . . . . . . . .498
Catecholamines . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .494
Cocaine, Ecgonine Methyl Ester . . . . . . . . . . . . . . . . .497
Nucleic Acid Bases . . . . . . . . . . . . . . . . . . . . . . . . . . .493
Opiates . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .496
System Suitability Mix . . . . . . . . . . . . . . . . . . . . . . . . .499
Allure® Aqueous C18 Columns (USP L1) Excellent Columns for LC/MS and ELSD Physical Characteristics:
pH range: 2.5 to 7.5temperature limit: 80°C
Chromatographic Properties:
Highly retentive and selective phase for separating polar analytes, including polar acidic compounds. Compatible with highly aqueous (up to 100%) mobile phases. Highly base deactivated. An excellent choice when analyzing a wide range of compounds, as in LC/MSscreening methods.
ordering
note
To order a 2.1mm, 3.2mm, or 4.6mm ID column with a Trident Integral Inlet Fitting, add “-700” to thecatalog number for the column.
Example: 100mm x 4.6mm ID Ultra C18 column with Trident Integral Inlet Fitting: 9174315-700
Also order an XG-XF fitting (cat.#25026 or 25062), see page 327.
available
For guard cartridges for these columns, see page 329.
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HPLC COLUMNS
Allure® Biphenyl Columns (USP L11) Physical Characteristics:
Application . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .Page #
Antibiotics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .526
Cannabinoids . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .496
Chromatographic Properties:
Corticosteroids . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .529
Highly retentive and selective for aromatic and unsaturated compounds. Increased retention
NSAIDs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .531
and selectivity, compared to phenyl phases. Excellent selectivity for steroids, tetracyclines,explosives, and other unsaturated compounds.
Steroids . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .529
Download your free copyfrom www.restek.com.
Allure® Organic Acids Columns Physical Characteristics:
pH range: 2.5 to 7.5temperature limit: 80°C
Chromatographic Properties:
Allure® Organic Acids columns provide enhanced retention and selectivity for polar organicacids, allowing the separation to be performed on a single 30cm column. An Allure® OrganicAcids column effectively resolves key organic acids such as tartaric and quinic acids, using thechromatographic conditions specified in AOAC method 986.13. Retention is stable and repro-ducible, even with the 100% aqueous mobile phase specified in the AOAC method.
Application . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .Page #
Carboxylic Acids . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .514
Fruit Juice Acids . . . . . . . . . . . . . . . . . . . . . . . . .514, 515
Note: Other dimensions available on request.
ordering
note
To order a 2.1mm, 3.2mm, or 4.6mm ID column with a Trident Integral Inlet Fitting, add “-700” to thecatalog number for the column.
Example: 100mm x 4.6mm ID Ultra C18 column with Trident Integral Inlet Fitting: 9174315-700
Also order an XG-XF fitting (cat.#25026 or 25062), see page 327.
For guard cartridges for these columns, see page 329.
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HPLC COLUMNS
Allure® Silica Columns (USP L3) Physical Characteristics:
pH range: 2.5 to 7.5temperature limit: 80°C
Chromatographic Properties:
Highly retentive phase for normal phase separations. Very high surface area, Type B silicapacking.
Allure® AK Columns
Physical Characteristics:
pH range: 2.5 to 7.5temperature limit: 80°C
Chromatographic Properties:
This highly retentive, highly selective phase, unique to Restek, was developed specifically forthe analysis of aldehydes and ketones as DNPH derivatives. Allure® AK is a reversed phaseHPLC material that has the unique ability to separate all thirteen carbonyl compounds speci-fied in California Air Resources Board (CARB) Method # 1004, using a simple acetonitrile/water gradient, in less than 15 minutes. Other columns require long analysis times or the useof tetrahydrofuran.
Application . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .Page #
5µm Columns with Trident Integral Inlet Fittings
Carbonyls . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .500
Carbonyls by CARB Method 1004 on an Allure® AK column.
Source: http://www.teknokroma.es/UserFiles/HPLC/Allure.pdf
En la ciudad de Concepción del Oro, municipio del mismo nombre del estado de Zacatecas, siendo las dieciséis horas del día seis de octubre de dos mil diez, se reunieron en la Sala de Cabildo de la Presidencia Municipal los CC. LIC. ROSA HUERTA BRIONES, PRESIDENTA MUNICIPAL, RICARDO ADRIAN URESTI LINARES, SINDICO MUNICIPAL, JULIO ABELARDO GONZALEZ PARDO, PROFRA. MINERVA CHAIREZ CRUZ, JOSE GUADA
Monte Carlo Simulation for Evaluation of Measurement Uncertainty of pharmaceutical certified reference materials Werickson Fortunato de Carvalho Rocha 1 , Raquel Nogueira2 1 INMETRO, Duque de Caxias, Brazil, [email protected] 2 INMETRO, Duque de Caxias , Brazil, [email protected] Abstract: The Supplemental Guide to the Expression of To avoid these limitations, t
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